1: 1.) magnesium / 1.) ether, 2.) ice-bath, 4 h
2: 1.) conc. HCl, sodium nitrite, 2.) sodium azide, sodium acetate / 1.) acetic acid, water, below 5 deg C
3: 49 percent / various solvent(s) / 3 h / Heating
4: various solvent(s) / 4 h / Heating
View Scheme
参考文献
Hawkins, David G.; Meth-Cohn, Otto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2077 - 2087
Agarwal, Rajesh; Chaudhary, Chapla; Misra, V. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 12 p. 1110 - 1113
Hawkins, David G.; Meth-Cohn, Otto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2077 - 2087