2-苯甲酰基氨基-4,5,6,7-四氢-1-苯并噻吩-3-羧酸合成路线 (共 6 条)
反应条件
thionyl chloride in N,N-dimethyl-formamide; benzene
0.333333 h; Heating;
参考文献
Kharizomenova, I.A.; Samsonova, N.V.; Kaplina, N.V.; Kapustina, M.V.; Grinev, A.N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 1 p. 36 - 37
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 1 p. 45 - 46
反应条件
sodium hydroxide in methanol
参考文献
Shvedov,V.I. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1973 , vol. 9, p. 1469 - 1472
Khimiya Geterotsiklicheskikh Soedinenii, 1973 , vol. 9, p. 1624 - 1627
反应条件
2: aq. NaOH / methanol
View Scheme
参考文献
Shvedov,V.I. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1973 , vol. 9, p. 1469 - 1472
Khimiya Geterotsiklicheskikh Soedinenii, 1973 , vol. 9, p. 1624 - 1627
反应条件
2: aq. NaOH / methanol
View Scheme
参考文献
Shvedov,V.I. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1973 , vol. 9, p. 1469 - 1472
Khimiya Geterotsiklicheskikh Soedinenii, 1973 , vol. 9, p. 1624 - 1627
反应条件
1: sulfur / Heating
2: water; sodium hydroxide
3: pyridine / 1 h / Cooling with ice
View Scheme
参考文献
Abdalha; El-Kassaby, M.K. Abou; El-Regal; Ali
Synthetic Communications, 2011 , vol. 41, # 19 p. 2811 - 2821
反应条件
pyridine
1 h; Cooling with ice;
参考文献
Abdalha; El-Kassaby, M.K. Abou; El-Regal; Ali
Synthetic Communications, 2011 , vol. 41, # 19 p. 2811 - 2821