2,6-二甲基-2,5-环己二烯-1,4-二酮合成路线 (共 148 条)
反应条件
in toluene
1.5 h; Heating;
参考文献
Mori, Akira; Mametsuka, Hiroaki; Takeshita, Hitoshi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 2072 - 2077
反应条件
T=110°C; 1 h; HeatingIrradiation;
参考文献
Barton, Derek H.R.; Crich, David; Kretzschmar, Gerhard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 39 - 54
反应条件
hydrogenchloride in ethanol; water
18 h; Ambient temperature;
参考文献
Ueno
Pharmazie, 1984 , vol. 39, # 5 p. 355 - 356
参考文献
Hasegawa, Kan-ichi; Ueno, Yoshio
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 510 - 517
参考文献
Ried,W.; Dietrich,R.
Chemische Berichte, 1961 , vol. 94, p. 387 - 391
反应条件
hydroxylamine hydrochloride in ethanol
24 h; Heating;
参考文献
Rathore, R.; Kim, J. S.; Kochi, J. K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 19 p. 2675 - 2684
反应条件
sulfuric acid
1.) THF, -78 deg C -> 20 deg C , 1 h, 2.) -78 deg C -> 20 deg C; 20 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Wigal, Carl T.; McKinley, Jason D.; Coyle, Jennifer; Porter, Diane J.; Lehman, Daniel E.
Journal of Organic Chemistry, 1995 , vol. 60, # 26 p. 8421 - 8423
参考文献
Fichter; Mueller
Helvetica Chimica Acta, 1935 , vol. 18, p. 831,833, 838