in dichloromethane
under Ar, Ph3CBF4 and Fe complex mixed in solid state, at 0°C added CH2Cl2, kept for 100 h from -10 to 10°C; ppt. centrifuged, washed with hexane, dried at room temp. in vac.;
参考文献
Suenkel, Karlheinz; Nagel, Ulrich; Beck, Wolfgang
Journal of Organometallic Chemistry, 1983 , vol. 251, # 2 p. 227 - 244
Dunlop-Briere, Alexandre F.; Baird, Michael C.; Budzelaar, Peter H. M.
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17514 - 17527