1-溴-2-(甲氧基甲基)苯合成路线 （共 24 条）
反应条件
1: pyridine 2: aqueous H2SO4 View Scheme
参考文献
Mann; Stewart
Journal of the Chemical Society, 1954 , p. 2819,2824
反应条件
N-bromosuccinmide in tetrachloromethane 1 h; IrradiationReflux;
参考文献
Mayhoub, Abdelrahman S.; Talukdar, Arindam; Cushman, Mark
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3507 - 3510
反应条件
1: Pd(OAc)2; dppb; iPr2NEt / dimethylsulfoxide / 12 h / 100 °C 2: LAH / diethyl ether / 3 h / Heating View Scheme
参考文献
Nandi, Malay; Jin, Jian; RajanBabu
Journal of the American Chemical Society, 1999 , vol. 121, # 42 p. 9899 - 9900
反应条件
1.1: n-butyllithium / diethyl ether; hexane / 1 h / -65 °C / |Inert atmosphere 1.2: 1 h / -65 °C / |Inert atmosphere 2.1: hydrogenchloride / diethyl ether; hexane; water / |Inert atmosphere View Scheme
参考文献
Adamczyk-Wozniak, Agnieszka; Brzozka, Zbigniew; Dabrowski, Marek; Madura, Izabela D.; Scheidsbach, Roy; Tomecka, Ewelina; Zukowski, Kamil; Sporzynski, Andrzej
Journal of Molecular Structure, 2013 , vol. 1035, p. 190 - 197
反应条件
1: pyridine 2: aq.-ethanolic NaOH 3: LiAlH4; diethyl ether 4: SOBr2; pyridine; CHCl3 View Scheme
参考文献
Mann; Stewart
Journal of the Chemical Society, 1954 , p. 2819,2824
反应条件
n-butyllithium; phosphorus trichoride
参考文献
Letsinger et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1806
反应条件
n-butyllithium; diethyl ether
anschliessendes Behandeln mit CO2;
参考文献
Mann; Stewart
Journal of the Chemical Society, 1954 , p. 2819,2824
反应条件
n-butyllithium
1.) methylcyclohexane, from 0 deg C to 25 deg C, 20 h, 2.) methylcyclohexane, Et2O; Yield given. Multistep reaction;
参考文献
Screttas, Constantinos G.; Steele, Barry R.
Journal of Organic Chemistry, 1989 , vol. 54, # 5 p. 1013 - 1017
反应条件
Behandeln des Reaktionsgemisches mit festem CO2;
参考文献
Fuson; Freedman
Journal of Organic Chemistry, 1958 , vol. 23, p. 1161,1164
Full Text Show Details
Letsinger et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1806
参考文献
Mann; Stewart
Journal of the Chemical Society, 1954 , p. 2819,2824
