5,6-二溴环己-2-烯-1,4-二酮合成路线 （共 8 条）
反应条件
in ethanol; water 1.) heating, 2.) 0 deg C, overnight;
参考文献
Atkinson, Romily C.; Mare, Peter B. D. de la; Larsen, David S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 271 - 280
参考文献
Nef
American Chemical Journal, 1890 , vol. 12, p. 484
Journal fuer Praktische Chemie (Leipzig), 1890 , vol. <2> 42, p. 184
Full Text Show Details
Nef
Journal fuer Praktische Chemie (Leipzig), 1890 , vol. <2> 42, p. 182,185
反应条件
1.1: 82 percent / NaBH4 / diethyl ether; H2O 2.1: K2CO3 / 0 - 20 °C 2.2: 71 percent / Heating 3.1: 100 percent / NEt3; H2O / methanol View Scheme
参考文献
Trost, Barry M.
Chemistry - A European Journal, 2001 , vol. 7, # 8 p. 1619 - 1629
反应条件
bei staerkerem Erhitzen;
参考文献
American Chemical Journal, , vol. 12, p. 484
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 42, p. 184
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 42, p. 182,185
反应条件
1: 88 percent / aq. NaBH4 / diethyl ether / 2 h / Ambient temperature 2: 68 percent / pyridine / 12 h View Scheme
参考文献
Johnson; Miller
Journal of Organic Chemistry, 1995 , vol. 60, # 21 p. 6674 - 6675
反应条件
1: NaBH4 2: Et3N, DMAP / CH2Cl2 3: 92 percent / Ti(O-i-Pr)4, i-PrOH / 85 °C View Scheme
参考文献
Johnson; Miller
Journal of Organic Chemistry, 1995 , vol. 60, # 21 p. 6674 - 6675
反应条件
sulfuric acid in tetrachloromethane; diethyl ether
T=0°C;
参考文献
SLOAN-KETTERING INSTITUTE FOR CANCER RESEARCH; DJABALLAH, Hakim; ANTCZAK, Christophe
Patent: WO2010/129049 A1, 2010 ;
Location in patent: Page/Page column 147 ;
WO 2010/129049 A1
参考文献
Nef
American Chemical Journal, 1890 , vol. 12, p. 484
Journal fuer Praktische Chemie (Leipzig), 1890 , vol. <2> 42, p. 184
Full Text Show Details
Nef
Journal fuer Praktische Chemie (Leipzig), 1890 , vol. <2> 42, p. 182,185
