反应条件
1: 90 percent / sodium nitrite / H2O / 72 h / 85 °C
2: 34 percent / lithium aluminium hydride / diethyl ether; dibutyl ether / 4 h / Heating
3: tert-butyl hyponitrite, triethylamine / dimethyl ether / 1 h / -78 °C
4: hexane / -10 °C / other solvents, temperatures; Ea, log A, ΔH<*>, ΔS<*>, ET, ΔG<*>
View Scheme
参考文献
Hinsberg, William D.; Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 766 - 773
