1,2,3,4-四氢-1-萘酚合成路线 (共 211 条)
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / diethyl ether 2: sodium carbonate / toluene / 72 h / 40 °C / Enzymatic reaction View Scheme
参考文献
Merabet-Khelassi, Mounia; Houiene, Zahia; Aribi-Zouioueche, Louisa; Riant, Olivier
Tetrahedron Asymmetry, 2012 , vol. 23, # 11-12 p. 828 - 833
反应条件
lipase Amano PS30 in various solvent(s) Enzymatic reaction;
参考文献
Merlic; Walsh
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2265 - 2274
反应条件
in hexane Acylation; isobutylation; 18 h; Heating; Title compound not separated from byproducts;
参考文献
Yamada, Shinji; Katsumata, Hiroko
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9365 - 9373
反应条件
in benzene T=35°C; 2.5 h; Irradiationporcine pancreas lipase-catalyzed; microwave irradiation; ee investigated; Rate constantProduct distribution;
参考文献
Lin, Gialih; Lin, Wen-Yuan
Tetrahedron Letters, 1998 , vol. 39, # 24 p. 4333 - 4336
反应条件
in benzene 2.5 h; HeatingIrradiationporcine pancreas lipase-catalyzed; microwave irradiation; ee investigated; Rate constantProduct distribution;
参考文献
Lin, Gialih; Lin, Wen-Yuan
Tetrahedron Letters, 1998 , vol. 39, # 24 p. 4333 - 4336
反应条件
hydrogen in cyclohexane T=80°C; P=5175.52 Torr; 24 h;
参考文献
Komatsu; Sugino; Hagiwara
Proceedings of the Imperial Academy (Tokyo), 1930 , vol. 6, p. 194,196
反应条件
supercritical CO2; hydrogen; Rh on carbon T=49.85°C; Title compound not separated from byproducts;
参考文献
Mine, Eiichi; Haryu, Eiji; Arai, Kunio; Sato, Takafumi; Sato, Osamu; Sasaki, Akiyoshi; Rode, Chandrashekhar V.; Shirai, Masayuki
Chemistry Letters, 2005 , vol. 34, # 6 p. 782 - 783
反应条件
nafion entrapped within palladium in cyclohexane T=80°C; 2 h; Reflux; Kinetics;
参考文献
Shapiro, Leora; Avnir, David
ChemCatChem, 2013 , vol. 5, # 8 p. 2195 - 2198
反应条件
triphenylphosphine in tetrahydrofuran T=70°C; Mitsunobu coupling; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 13 p. 5012 - 5015
反应条件
tert.-butylhydroperoxide; chromium(VI) oxide in dichloromethane 6 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 28, # 19 p. 2133 - 2134