2-(3,4-二氯苯基)环氧乙烷合成路线 (共 9 条)
反应条件
Product distribution;
参考文献
Fuchs
Journal of the American Chemical Society, 1956 , vol. 78, p. 5612
反应条件
Hydrogenation; Product distribution;
参考文献
Park; Fuchs
Journal of Organic Chemistry, 1957 , vol. 22, p. 93
反应条件
Product distribution;
参考文献
Fuchs
Journal of the American Chemical Society, 1956 , vol. 78, p. 5612
反应条件
Hydrogenation; Product distribution;
参考文献
Park; Fuchs
Journal of Organic Chemistry, 1957 , vol. 22, p. 93
反应条件
1,4-dioxane; anhydrous sodium borate
Erwaermen einer Loesung des erhaltenen 2-Brom-1-<3,4-dichlor-phenyl>-aethanols in Diisopropylaether mit wss. Kalilauge;
参考文献
Fuchs
Journal of the American Chemical Society, 1956 , vol. 78, p. 5612
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=0 - 20°C; 15 h;
参考文献
Efange, Simon M. N.; Kamath, Ashok P.; Khare, Anil B.; Kung, Mei-Ping; Mach, Robert H.; Parsons, Stanley M.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 24 p. 3905 - 3914
反应条件
1: 68 percent / TsOH / benzene / 4 h
2: 3-chloroperbenzoic acid / CH2Cl2 / 15 h / 0 - 20 °C
View Scheme
参考文献
Efange, Simon M. N.; Kamath, Ashok P.; Khare, Anil B.; Kung, Mei-Ping; Mach, Robert H.; Parsons, Stanley M.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 24 p. 3905 - 3914
反应条件
1: 89 percent / NaBH4 / methanol / 1 h / Ambient temperature
2: 68 percent / TsOH / benzene / 4 h
3: 3-chloroperbenzoic acid / CH2Cl2 / 15 h / 0 - 20 °C
View Scheme
参考文献
Efange, Simon M. N.; Kamath, Ashok P.; Khare, Anil B.; Kung, Mei-Ping; Mach, Robert H.; Parsons, Stanley M.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 24 p. 3905 - 3914
参考文献
Cavalleri,B.; Bellasio,E.
Farmaco, Edizione Scientifica, 1970 , vol. 25, p. 901 - 911