反应条件
1: 10 palladium on activated charcoal; hydrogen / ethanol 2: toluene-4-sulfonic acid; trimethyl orthoformate / dichloromethane / 20 °C 3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / Cooling with ice 4: sodium methylate / methanol; dichloromethane 5: methanesulfonic acid / methanol; water / 0.25 h View Scheme
参考文献
Hamilton, Niall M.; Dawson, Martin; Fairweather, Emma E.; Hamilton, Nicola S.; Hitchin, James R.; James, Dominic I.; Jones, Stuart D.; Jordan, Allan M.; Lyons, Amanda J.; Small, Helen F.; Thomson, Graeme J.; Waddell, Ian D.; Ogilvie, Donald J.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 9 p. 4431 - 4445
