去氢表雄酮合成路线

参考文献

Miescher; Wettstein
Helvetica Chimica Acta, 1938 , vol. 21, p. 1317,1322
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Kuwada; Miyasaka
Yakugaku Zasshi, 1937 , vol. 57, p. 459,463;dtsch.Ref.S.96
Chem. Zentralbl., 1937 , vol. 108, # II p. 1825
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Schering A.G.
Patent: DE657017 , 1935 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 24, p. 497

64-17-5乙醇+

53-43-0去氢表雄酮+

151-50-8氰化钾+

64-19-7醋酸

35060-03-8

参考文献

Butenandt; Schmidt-Thome
Chemische Berichte, 1938 , vol. 71, p. 1487,1490
Chemische Berichte, 1939 , vol. 72, p. 182,185

参考文献

Kuwada; Miyasaka
Yakugaku Zasshi, 1937 , vol. 57, p. 459,463;dtsch.Ref.S.96
Chem. Zentralbl., 1937 , vol. 108, # II p. 1825

53-43-0去氢表雄酮+

1066-54-2三甲基乙炔基硅

3604-60-217-乙炔基-10,13-二甲基-1,2,3,4,7,8,9,11,12,14,15,16-十二氢环戊烯并[a]菲-3,17-二醇

参考文献

Wong, Fung Fuh; Chuang, Shih Hsien; Yang, Sheng-chuan; Lin, Yu-Hsiang; Tseng, Wen-Che; Lin, Shao-Kai; Huang, Jiann-Jyh
Tetrahedron, 2010 , vol. 66, # 23 p. 4068 - 4072

53-43-0去氢表雄酮+

74-86-2乙炔

3604-60-217-乙炔基-10,13-二甲基-1,2,3,4,7,8,9,11,12,14,15,16-十二氢环戊烯并[a]菲-3,17-二醇

参考文献

Stavely
Journal of the American Chemical Society, 1939 , vol. 61, p. 79
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Sondheimer et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 1742
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Squibb and Sons
Patent: US2239864 , 1938 ;

53-43-0去氢表雄酮+

70277-75-7

3604-60-217-乙炔基-10,13-二甲基-1,2,3,4,7,8,9,11,12,14,15,16-十二氢环戊烯并[a]菲-3,17-二醇

参考文献

Schor, Laura; Seldes, Alicia M.; Gros, Eduardo G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 163 - 166

53-43-0去氢表雄酮+

1066-26-8乙炔钠

3604-60-217-乙炔基-10,13-二甲基-1,2,3,4,7,8,9,11,12,14,15,16-十二氢环戊烯并[a]菲-3,17-二醇

参考文献

Marwah, Padma; Marwah, Ashok; Lardy, Henry A.; Miyamoto, Hiroshi; Chang, Chawnshang
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 17 p. 5933 - 5947

53-43-0去氢表雄酮+

74-86-2乙炔

参考文献

Sondheimer et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 1742

53-43-0去氢表雄酮+

1111-63-3乙炔钾

3604-60-217-乙炔基-10,13-二甲基-1,2,3,4,7,8,9,11,12,14,15,16-十二氢环戊烯并[a]菲-3,17-二醇

参考文献

Ciba
Patent: DE702063 , 1938 ;
DRP/DRBP Org.Chem.
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Reichstein; Meystre
Helvetica Chimica Acta, 1939 , vol. 22, p. 728,737
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Kathol; Logemann; Serini
Naturwissenschaften, 1937 , vol. 25, p. 682
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Ciba
Patent: CH202847 , 1937 ;

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Ciba Pharm. Prod. Inc.
Patent: US2267257 , 1938 ;

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Ruzicka; Hofmann
Helvetica Chimica Acta, 1937 , vol. 20, p. 1280

53-43-0去氢表雄酮+

1111-63-3乙炔钾

3604-60-217-乙炔基-10,13-二甲基-1,2,3,4,7,8,9,11,12,14,15,16-十二氢环戊烯并[a]菲-3,17-二醇+

102571-56-2

参考文献

Reichstein; Meystre
Helvetica Chimica Acta, 1939 , vol. 22, p. 728,737