反应条件
in cyclohexane Kinetics; Irradiation (UV/VIS); under N2, soln. of W(CO)5CPh2 in C6H12 added to soln. of alkene in C6H12, irradiated through Pyrex filter at 25.+-.1°C for 4 h / kinetics monitored at 12-14 and 27-29°C by UV; concd. in vac., extd. with cold pentane (-10°C), evapd., redissolved in CCl4, chromd. (SiO2/deactivated with H2O, CCl4, -15°C), collected at 0°C, evapd. in vac., dissolved in pentane, evapd. in vac.; elem. anal.;
参考文献
Fong,L.K.; Cooper,N.J.
Journal of the American Chemical Society, 1984 , vol. 106, p. 2595
