1-(5-氯-2-硝基苯基)哌啶合成路线 (共 7 条)
反应条件
in ethanol T=0 - 23°C; 0.75 h;
参考文献
WO2006/47504 A1, ;
Page/Page column 39 ;
WO 2006/047504 A1
反应条件
triethylamine in 1,4-dioxane T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 51, # 4 p. 641 - 644
反应条件
in methanol T=20°C; 5 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 40, # 10 p. 1473 - 1476
参考文献
Gazzetta Chimica Italiana, , vol. 63, p. 612,620
Journal of the American Chemical Society, , vol. 62, p. 750,754
反应条件
triethylamine in dimethyl sulfoxide T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 51, # 4 p. 641 - 644
反应条件
1: KNO3; concentrated H2SO4 2: ethanol View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 63, p. 612,620
参考文献
Journal of the American Chemical Society, , vol. 62, p. 750,754