4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
boron trifluoride diethyl etherate; palladium diacetate in methanol T=20°C; 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 9 p. 1654 - 1658
反应条件
zinc(II) chloride; 3-Cl-pyridine-Pd-{CH-[N-(2,6-di-iPrC6H3)CH]2}Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=20°C; Negishi cross-coupling reaction; 24 h;
参考文献
Chemistry - A European Journal, , vol. 12, # 18 p. 4749 - 4755
反应条件
1: 87 percent / pyridine / CHCl3 / 12 h / 20 °C 2: 60 percent / dppfNiCl2 / tetrahydrofuran / 28 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 8 p. 3017 - 3025
反应条件
1: 90 percent / phosphate buffer / Pd/C / dioxane / 3 h / 20 °C / pH 6.84 2: 81 percent / Ag2O; Pd(PPh3)4 / tetrahydrofuran / 12 h / 60 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 17 p. 5342 - 5349
反应条件
palladium 10 on activated carbon in methanol Suzuki-Miyaura cross-coupling; RefluxUnder air;
参考文献
Letters in Organic Chemistry, , vol. 7, # 1 p. 1 - 6
反应条件
in tetrahydrofuran T=110°C; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 35 p. 7891 - 7894
反应条件
1: 94 percent / pyridine / 12 h / 20 °C 2: 92 percent / Pd(dba)2; 2-dicyclohexylphosphinobiphenyl; TBAF / tetrahydrofuran / 6 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 4 p. 1137 - 1143
反应条件
1: para-bromotoluene With magnesium in diethyl ether 2: 1-bromo-4-methoxy-benzene in diethyl ether Kumada coupling reaction; 3 h; Reflux;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 2 p. 331 - 335
反应条件
tBu2P-N=P(iBuPCH2CH2)3N; tetrabutyl ammonium fluoride; palladium diacetate T=80°C; Hiyama coupling; 2 h; Inert atmosphereNeat (no solvent);
参考文献
Journal of Organic Chemistry, , vol. 75, # 5 p. 1744 - 1747
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; n-butyllithium; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in toluene T=100°C; 16 h; various reaction conditions; Product distribution;
参考文献
Tetrahedron, , vol. 54, # 43 p. 13079 - 13086