3,3-二甲基戊烷-1,5-二醇合成路线 （共 18 条）
反应条件
1: SOCl2 3: concentrated H2SO4 4: aqueous Ba(OH)2-solution View Scheme
参考文献
Miller; Adams
Journal of the American Chemical Society, 1936 , vol. 58, p. 787,789
反应条件
ruthenium(IV) oxide; sodium chloride in tetrachloromethane; water electrooxidation;
参考文献
Torii, Sigeru; Inokuchi, Tsutomu; Sugiura, Toyoyuki
Journal of Organic Chemistry, 1986 , vol. 51, # 2 p. 155 - 161
反应条件
1: sulfuric acid; hydrobromic acid; water 2: ethanol View Scheme
参考文献
Miller; Adams
Journal of the American Chemical Society, 1936 , vol. 58, p. 787,789
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether
1) 2 h, reflux, 2) 12 h, r.t.;
参考文献
Eilbracht, Peter; Acker, Michael; Totzauer, Walter
Chemische Berichte, 1983 , vol. 116, # 1 p. 238 - 242
反应条件
sulfuric acid; sodium hydrogencarbonate in methanol; water; 1,2-dichloro-ethane
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5958942 A1, 1999 ;
反应条件
sulfuric acid in methanol; water; 1,2-dichloro-ethane
参考文献
Takeda Chemical Industries Ltd.
Patent: US5840732 A1, 1998 ;
参考文献
Ryhage; Stenhagen
Arkiv foer Kemi, 1959 , vol. 14, p. 483,484
反应条件
lithium aluminium tetrahydride in diethyl ether
Heating;
参考文献
Miller,R.G. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 4211 - 4220
反应条件
1.1: CuI / tetrahydrofuran / 20 °C
1.2: TMSCl / tetrahydrofuran / -78 - 20 °C
2.1: lithium aluminum hydride / tetrahydrofuran / 24 h / Heating
View Scheme
参考文献
Chang, Chih-Shiang; Lin, Ying-Ting; Shih, Shin-Ru; Lee, Chung-Chi; Lee, Yen-Chun; Tai, Chia-Liang; Tseng, Sung-Nien; Chern, Jyh-Haur
Journal of Medicinal Chemistry, 2005 , vol. 48, # 10 p. 3522 - 3535
反应条件
1: aq. H2SO4
2: aq. H2SO4
3: LiAlH4 / diethyl ether
View Scheme
参考文献
Handley,G.J. et al.
Australian Journal of Chemistry, 1960 , vol. 13, p. 129 - 144
