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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴-6-甲基吡啶
合成路线
（共 135 条）
5315-25-3
2-溴-6-甲基吡啶
+
3430-17-9
2-溴-3-甲基吡啶
→
反应条件
109-06-8
2-甲基吡啶
+
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
108-99-6
3-甲基吡啶
+
947331-94-4
+
1762-32-9
3,3-二甲基-2,2-联吡啶
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
5315-25-3
2-溴-6-甲基吡啶
→
反应条件
109-06-8
2-甲基吡啶
+
4411-80-7
6,6′-二甲基-2,2′-联吡啶
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride in methylbutan-2-ol T=100°C; 18 h; Inert atmosphere;
参考文献
Zeng, Minfeng; Du, Yijun; Shao, Linjun; Qi, Chenze; Zhang, Xian-Man
Journal of Organic Chemistry, 2010 , vol. 75, # 8 p. 2556 - 2563
5315-25-3
2-溴-6-甲基吡啶
+
259807-95-9
2-甲基-6-(三丁基锡)吡啶
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Stille-type cross-coupling; 48 h; Heating;
参考文献
Heller, Marcel; Schubert, Ulrich S.
Journal of Organic Chemistry, 2002 , vol. 67, # 23 p. 8269 - 8272
5315-25-3
2-溴-6-甲基吡啶
+
95-16-9
苯并噻唑
→
反应条件
22201-26-9
+
4411-80-7
6,6′-二甲基-2,2′-联吡啶
反应条件
PdCl(C3H5)(dppb); caesium carbonate in N,N-dimethyl-formamide T=150°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Derridj, Fazia; Gottumukkala, Aditya L.; Djebbar, Safia; Doucet, Henri
European Journal of Inorganic Chemistry, 2008 , # 16 p. 2550 - 2559
96-43-5
2-氯噻吩
+
5315-25-3
2-溴-6-甲基吡啶
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
1062177-19-8
反应条件
PdCl(C3H5)(dppb); potassium acetate in N,N-dimethyl acetamide T=150°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Derridj, Fazia; Gottumukkala, Aditya L.; Djebbar, Safia; Doucet, Henri
European Journal of Inorganic Chemistry, 2008 , # 16 p. 2550 - 2559
4466-24-4
2-正丁基呋喃
+
5315-25-3
2-溴-6-甲基吡啶
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
1062177-16-5
反应条件
PdCl(C3H5)(dppb); potassium acetate in N,N-dimethyl acetamide T=150°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Derridj, Fazia; Gottumukkala, Aditya L.; Djebbar, Safia; Doucet, Henri
European Journal of Inorganic Chemistry, 2008 , # 16 p. 2550 - 2559
1455-20-5
2-正丁基噻吩
+
5315-25-3
2-溴-6-甲基吡啶
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
1062177-17-6
反应条件
PdCl(C3H5)(dppb); potassium acetate in N,N-dimethyl acetamide T=150°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Derridj, Fazia; Gottumukkala, Aditya L.; Djebbar, Safia; Doucet, Henri
European Journal of Inorganic Chemistry, 2008 , # 16 p. 2550 - 2559
5315-25-3
2-溴-6-甲基吡啶
+
1632-83-3
1-甲基苯并咪唑
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
143266-97-1
反应条件
PdCl(C3H5)(dppb); potassium acetate in N,N-dimethyl acetamide T=150°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Derridj, Fazia; Gottumukkala, Aditya L.; Djebbar, Safia; Doucet, Henri
European Journal of Inorganic Chemistry, 2008 , # 16 p. 2550 - 2559
5315-25-3
2-溴-6-甲基吡啶
+
562086-28-6
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
562086-30-0
反应条件
1: 2-bromo-6-methyl-pyridine With n-butyllithium; tributyltin chloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: methyl 2-methyl-6-lt;(p-toluenesulfonyl)oxygt;pyridine-4-carboxylate With triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in xylene Stille-type cross-coupling; 24 h; Heating;
参考文献
Mathieu, Julien; Marsura, Alain
Synthetic Communications, 2003 , vol. 33, # 3 p. 409 - 414
5315-25-3
2-溴-6-甲基吡啶
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
562086-30-0
反应条件
1: 2-bromo-6-methyl-pyridine With n-butyllithium; tributyltin chloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: 4-carbomethoxy-6-methyl-2-(methanesulfonyloxy)pyridine With triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in xylene Stille-type cross-coupling; 24 h; Heating;
参考文献
Mathieu, Julien; Marsura, Alain
Synthetic Communications, 2003 , vol. 33, # 3 p. 409 - 414
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