1-(1,3-二噻烷-2-基)-2-环己烯-1-醇合成路线 （共 6 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in tetrahydrofuran
T=-78°C;
参考文献
O'Neil, Ian A.; Lai, Justine Y. Q.; Wynn, Duncan
Chemical Communications, 1999 , # 1 p. 59 - 60
反应条件
n-butyllithium in tetrahydrofuran; hexane
1.) -10 deg C, 2 h, 2.) 0 deg C, 18 h;
参考文献
Ranu, Brindaban C.; Sarkar, Dipak C.
Synthetic Communications, 1987 , vol. 17, # 2 p. 155 - 160
反应条件
ligand (4a) in tetrahydrofuran
T=-78°C;
参考文献
Wilson, Stephen R.; Price, Martyn F.
Synthetic Communications, 1982 , vol. 12, # 9 p. 657 - 664
反应条件
chiral urea C20H24N2O in tetrahydrofuran
T=-78°C; 4 h;
参考文献
Juaristi, Eusebio; Hernandez-Rodriguez, Marcos; Lopez-Ruiz, Heraclio; Avina, Judit; Munoz-Muniz, Omar; Hayakawa, Michiya; Seebach, Dieter
Helvetica Chimica Acta, 2002 , vol. 85, # 7 p. 1999 - 2008
反应条件
n-butyllithium
1.) THF, hexane, RT, 1 h, 2.) THF, RT, overnight; Yield given. Multistep reaction;
参考文献
Ager, David J.; East, Michael B.
Journal of Organic Chemistry, 1986 , vol. 51, # 21 p. 3983 - 3992
反应条件
tetrafluoroboric acid; mercury(II) oxide in tetrahydrofuran; water
3 h; Heating;
参考文献
Ranu, Brindaban C.; Sarkar, Dipak C.
Synthetic Communications, 1987 , vol. 17, # 2 p. 155 - 160
