NaOH in water; acetonitrile to aq. soln. of acid aq. soln. of NaOH added with stirring, then soln. of AgNO3 in CH3CN added under stirring; soln. slowly evapd. in air for 48 h, ppt. filtered, washed (H2O), dried (avc.); elem. anal.;
参考文献
Liu, Xiu-Ying; Zhu, Hai-Liang
Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2005 , vol. 35, # 2 p. 155 - 159
in water dropwise addn. of a satd. aq. soln. of AgNO3 to an aq. soln. of ammonium benzoate; pptn., cooling in ice, filtration, washing (cold water, cold ethanol, ether), drying by suction;
参考文献
Anderson, Gordon K.; Lumetta, Gregg J.
Inorganic Chemistry, 1987 , vol. 26, p. 1291 - 1295
diethyl ether Erhitzen des Reaktionsprodukts auf 80-100grad;
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1901 , vol. 318, p. 20
Full Text Show Details
Silva
Bulletin de la Societe Chimique de France, 1869 , vol. <2> 12, p. 224
Hamonet
Bulletin de la Societe Chimique de France, 1905 , vol. <3>33, p. 526
Full Text Show Details
Fichter; Schnider
Helvetica Chimica Acta, 1931 , vol. 14, p. 860