1: With ethyl bromide; magnesium in tetrahydrofuran
T=50°C; Inert atmosphereReflux;
2: acetylene in tetrahydrofuran
T=50°C; Inert atmosphereReflux;
3: cyclopentanone in tetrahydrofuran
2 h; Inert atmosphereReflux;
参考文献
Fallon, Thomas; Robinson, Diane E.J.E.; Willis, Anthony C.; Paddon-Row, Michael N.; Sherburn, Michael S.
Chemistry - A European Journal, 2010 , vol. 16, # 3 p. 760 - 765
Pinkney; Marvel
Journal of the American Chemical Society, 1937 , vol. 59, p. 2669,2671
Full Text Show Details
Salkind; Gwerdziteli
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 855,861
Chem. Zentralbl., 1939 , vol. 110, # II p. 3803
Pinkney; Marvel
Journal of the American Chemical Society, 1937 , vol. 59, p. 2669,2671
Full Text Show Details
Salkind; Gwerdziteli
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 855,861
Chem. Zentralbl., 1939 , vol. 110, # II p. 3803
Pinkney; Marvel
Journal of the American Chemical Society, 1937 , vol. 59, p. 2669,2671
Full Text Show Details
Salkind; Gwerdziteli
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 855,861
Chem. Zentralbl., 1939 , vol. 110, # II p. 3803
trichlorophosphate in pyridine
T=100°C; 0.5 h; Inert atmosphere;
参考文献
Fallon, Thomas; Robinson, Diane E.J.E.; Willis, Anthony C.; Paddon-Row, Michael N.; Sherburn, Michael S.
Chemistry - A European Journal, 2010 , vol. 16, # 3 p. 760 - 765
