1-(2-(烯丙氧基)苯基)乙酮合成路线 （共 18 条）
反应条件
1: 52 percent / K2CO3; tetrabutylammonium bromide / benzene; H2O / 16 h / Heating
2: 28 percent / BuLi; HMPA / tetrahydrofuran / -78 - 5 °C
View Scheme
参考文献
Nikitin, Kirill V.; Andryukhova, Nonna P.
Canadian Journal of Chemistry, 2004 , vol. 82, # 5 p. 571 - 578
反应条件
silica gel
0.25 h; microwave irradiation;
参考文献
Singh, Surinderjit; Ishar; Singh, Gajendra; Singh, Rajinder
Canadian Journal of Chemistry, 2005 , vol. 83, # 3 p. 260 - 265
反应条件
in toluene
72 h; Heating;
参考文献
Singh, Surinderjit; Ishar; Singh, Gajendra; Singh, Rajinder
Canadian Journal of Chemistry, 2005 , vol. 83, # 3 p. 260 - 265
反应条件
1: 45 percent / p-TsOH / toluene / 22 h / Heating
2: 3 percent / 650 °C / 0.01 Torr
View Scheme
参考文献
Black, Michael; Cadogan; Leardini, Rino; McNab, Hamish; McDougald, Graham; Nanni, Daniele; Reed, David; Zompatori, Alberto
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 11 p. 1825 - 1832
反应条件
1: LDA / tetrahydrofuran; hexane / 2 h / -78 °C
2: (PCy3)Cl2Ru(=CHPh)[-CHN(Mes)CH2CH2N(Mes)-] / benzene / 1 h / 65 °C
View Scheme
参考文献
Okada, Akihiro; Ohshima, Takashi; Shibasaki, Masakatsu
Tetrahedron Letters, 2001 , vol. 42, # 45 p. 8023 - 8027
反应条件
lithium diisopropyl amide in tetrahydrofuran
参考文献
Whitehead, Alan; Moore, Joel D.; Hanson, Paul R.
Tetrahedron Letters, 2003 , vol. 44, # 22 p. 4275 - 4277
反应条件
T=200°C; Claisen rearrangement; 44 h;
参考文献
ROWETT RESEARCH INSTITUTE
Patent: WO2004/7475 A1, 2004 ;
Location in patent: Page 103-104 ;
反应条件
ytterbium(III) triflate in acetonitrile
Substitution; Claisen rearrangement; 72 h; Heating;
参考文献
Sharma; Ilangovan; Sreenivas, Punna; Mahalingam
Synlett, 2000 , # 5 p. 615 - 618
