3-(3,4-二甲氧基苯甲酰)丙酸合成路线 (共 32 条)
反应条件
AlCl3, aluminium chloride in nitrobenzene T=0 - 60°C; 3 h;
参考文献
Council of Scientific and Industrial Research
Patent: US2004/14993 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
hydrogenchloride in acetic acid
参考文献
Cytomed, Inc.
Patent: US5681966 A1, 1997 ;
US 5681966 A
反应条件
hydrogenchloride; AlCl3
参考文献
Fanto, Nicola; Tinti, Maria Ornella
Patent: US2003/195257 A1, 2003 ;
反应条件
1: 1-(3,4-dimethoxyphenyl)-1-N-morpholinoacetonitrile With sodium hydride in N,N-dimethyl-formamide T=0°C; 0.5 h; 2: acrylic acid methyl ester in N,N-dimethyl-formamide T=0 - 20°C;
参考文献
Pawar; Waghmare; Lokhande
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 11 p. 2549 - 2551
反应条件
sodium hydroxide 0.166667 h; Heating;
参考文献
Fetter, J.; Lempert, K.; Moeller, J.; Nyitrai, J.; Zauer, K.
Acta Chimica Hungarica, 1983 , vol. 112, # 1 p. 43 - 58
反应条件
1: 85 percent / aq. KOH / ethanol / 2 h / Heating 2: methanol; H2O / 0.5 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 116, # 1 p. 220 - 229
反应条件
1: AlCl3 / chlorobenzene / 1.) below 2 deg C 2.) 0 deg C, 1/2 h 3.) rt., 1 h 2: 91.5 percent / 2 N NaOH / 0.17 h / Heating View Scheme
参考文献
Acta Chimica Hungarica, , vol. 112, # 1 p. 43 - 58
反应条件
in methanol; water 0.5 h; Heating; Yield given;
参考文献
Chemische Berichte, , vol. 116, # 1 p. 220 - 229
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 242, p. 2956
参考文献
Gazzetta Chimica Italiana, , vol. 42 I, p. 205