1,2,3,5-四甲氧基苯合成路线 （共 92 条）
反应条件
aluminium trichloride in diethyl ether
T=22°C; 2 h;
参考文献
Rizzi, George P.
Synthetic Communications, 1983 , vol. 13, # 14 p. 1173 - 1180
参考文献
Horton,W.J.; Stout,M.G.
Journal of Organic Chemistry, 1962 , vol. 27, p. 830 - 833
反应条件
aluminium trichloride
参考文献
Nierenstein
Journal of the Chemical Society, 1917 , vol. 111, p. 9
Show Details
Bargellini; Bini
Gazzetta Chimica Italiana, 1911 , vol. 41 II, p. 17
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1910 , vol. <5> 19 II, p. 599
反应条件
In(OSO2CF3)3
T=85 - 95°C; Friedel-Crafts acetylation; 0.05 h; IrradiationMicrowave;
参考文献
Tsukayama, Masao; Kusunoki, Eiji; Hossain, Mohammad M.; Kawamura, Yasuhiko; Hayashi, Shinji
Heterocycles, 2007 , vol. 71, # 7 p. 1589 - 1600
反应条件
1: 1.38 g / AlCl3 / diethyl ether / 2 h / 22 °C
2: 84 percent / K2CO3 / acetone / 17 h / Heating
View Scheme
参考文献
Asakawa, Tomohiro; Hiza, Aiki; Nakayama, Miho; Inai, Makoto; Oyama, Dai; Koide, Hiroyuki; Shimizu, Kosuke; Wakimoto, Toshiyuki; Harada, Norihiro; Tsukada, Hideo; Oku, Naoto; Kan, Toshiyuki
Chemical Communications, 2011 , vol. 47, # 10 p. 2868 - 2870
参考文献
Gardner et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 2541
反应条件
aluminium trichloride in diethyl ether
T=22°C; 2 h;
参考文献
Rizzi, George P.
Synthetic Communications, 1983 , vol. 13, # 14 p. 1173 - 1180
反应条件
In(OSO2CF3)3
T=75 - 90°C; 0.1 h; microwave irradiation;
参考文献
Tsukayama, Masao; Kawamura, Yasuhiko; Ishizuka, Takaaki; Hayashi, Shinji; Torii, Fumihito
Heterocycles, 2003 , vol. 60, # 12 p. 2775 - 2784
参考文献
Chapman; Perkin; Robinson
Journal of the Chemical Society, 1927 , p. 3020
Show Details
Bargellini; Bini
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1910 , vol. <5> 19 II, p. 598
Gazzetta Chimica Italiana, 1911 , vol. 41 II, p. 17
反应条件
1: AlCl3; diethyl ether
2: sodium-<4-methoxy benzoate> / 180 °C
View Scheme
参考文献
Wessely; Kallab
Monatshefte fuer Chemie, 1932 , vol. 60, p. 26,30
