D-(+)-核糖酸-1,4-内酯合成路线 (共 50 条)
反应条件
1: 98 percent / aq. HCl / 7 h / Ambient temperature 2: 1.) NaH 3: 93 percent / n-Bu3SnH, AIBN / toluene / Heating 4: 96 percent / TFA / H2O; CHCl3 / 10 h / 70 °C View Scheme
参考文献
Shin Yih Chen; Joullie
Tetrahedron Letters, 1983 , vol. 24, # 46 p. 5027 - 5030
反应条件
boron trifluoride diethyl etherate in tetrahydrofuran 7 h; Ambient temperature;
参考文献
Miller, Scott A.; Chamberlin, A. Richard
Journal of the American Chemical Society, 1990 , vol. 112, # 22 p. 8100 - 8112
反应条件
Sikkon; iron(III) chloride T=50°C; 2.5 h;
参考文献
Beer; Meuwly; Vasella
Helvetica Chimica Acta, 1982 , vol. 65, # 8 p. 2570 - 2582
反应条件
hydrogen cation in acetone
参考文献
Obayashi, Michio; Schlosser, Manfred
Chemistry Letters, 1985 , p. 1715 - 1718
参考文献
Damont, Annelaure; Dukhan, David; Gosselin, Gilles; Peyronnet, Jerome; Storer, Richard
Nucleosides, Nucleotides and Nucleic Acids, 2007 , vol. 26, # 10-12 p. 1431 - 1434
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=0°C; 5 h;
参考文献
Bennis, Khalil; Calinaud, Pierre; Gelas, Jacques; Ghobsi, Mebrouk
Carbohydrate Research, 1994 , vol. 264, # 1 p. 33 - 44
反应条件
toluene-4-sulfonic acid T=25°C; 24 h;
参考文献
Tetrahedron, , vol. 53, # 4 p. 1311 - 1322
反应条件
hydrogenchloride 20 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 49, # 2 p. 349 - 362
反应条件
hydrogenchloride; acetone
参考文献
Hough et al.
Canadian Journal of Chemistry, 1958 , vol. 36, p. 1720,1725
反应条件
toluene-4-sulfonic acid 48 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 53, # 36 p. 12067 - 12088