2-(苯甲酰基)丁酸甲酯合成路线 (共 10 条)
反应条件
Wilkinson's catalyst; (Z,Z)-1,5-cyclooctadiene; diethylzinc in tetrahydrofuran; hexane
T=0°C; Reformatsky-Honda Reaction; 1 h; Inert atmosphere;
参考文献
Sato, Kazuyuki; Isoda, Motoyuki; Ohata, Shizuka; Morita, Shuhei; Tarui, Atsushi; Omote, Masaaki; Kumadaki, Itsumaro; Ando, Akira
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 510 - 514
反应条件
anhydrous butyl ether; sodium hydride
参考文献
Swamer; Hauser
Journal of the American Chemical Society, 1950 , vol. 72, p. 1352,1353, 1356
反应条件
methanol; titanium tetrachloride in dichloromethane
addition of reagents at -78 deg C, 2 h; reaction at room temperature;
参考文献
Reddy, Chaganti P.; Tanimoto, Shigeo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 411 - 414
反应条件
1: sodium amide; liquid ammonia / Eintragen des Reaktionsgemisches in festes Kohlendioxid
2: diethyl ether
View Scheme
参考文献
Levine; Hauser
Journal of the American Chemical Society, 1944 , vol. 66, p. 1768
参考文献
Levine; Hauser
Journal of the American Chemical Society, 1944 , vol. 66, p. 1768
反应条件
Jones reagent in acetone
参考文献
Taniguchi, Masahiko; Fujii, Hideaki; Oshima, Koichiro; Utimoto, Kiitiro
Tetrahedron, 1993 , vol. 49, # 48 p. 11169 - 11182
反应条件
2: CrO3 in H2SO4 / acetone
View Scheme
参考文献
Taniguchi, Masahiko; Fujii, Hideaki; Oshima, Koichiro; Utimoto, Kiitiro
Tetrahedron, 1993 , vol. 49, # 48 p. 11169 - 11182
反应条件
2: CrO3 in H2SO4 / acetone
View Scheme
参考文献
Taniguchi, Masahiko; Fujii, Hideaki; Oshima, Koichiro; Utimoto, Kiitiro
Tetrahedron, 1993 , vol. 49, # 48 p. 11169 - 11182
反应条件
in dichloromethane
Ambient temperature;
参考文献
Reddy, Chaganti P.; Tanimoto, Shigeo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 411 - 414
参考文献
Royals
Journal of the American Chemical Society, 1948 , vol. 70, p. 489