1-(4-甲氧苯基)丙烷-1-OL合成路线 (共 45 条)
反应条件
1: AlCl3; petroleum ether / man zersetzt die oelige Doppelverbindung mit Eis 2: sodium; ethanol View Scheme
参考文献
Chemische Berichte, , vol. 35, p. 2263
Chemische Berichte, , vol. 38, p. 913
反应条件
C6mim(1+)Br(1-) T=140°C; 0.116667 h; Microwave irradiationCombinatorial reaction / High throughput screening (HTS); Reactivity; Reagent/catalystTime; chemoselective reaction;
参考文献
Kumar, Rakesh; Sharma, Abhishek; Sharma, Naina; Kumar, Vinod; Sinha, Arun K.
European Journal of Organic Chemistry, 2008 , # 33 p. 5577 - 5582
反应条件
toluene-4-sulfonic acid in benzene Heating; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1480 - 1492
反应条件
1: HBr / 0 °C 2: diethyl ether; sodium 3: aqueous HI; acetic acid View Scheme
参考文献
Sah
Journal of the Chinese Chemical Society (Peking), 1946 , vol. 13, p. 111,117
反应条件
n-butyllithium; titanium(III) chloride; triethylamine 1.) hexane, 1,2-dimethoxyethane; 2.) room temp., 2 h; reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schloegl, Karl; Weissensteiner, Walter
Synthesis, 1982 , # 1 p. 50 - 53
反应条件
T=120°C; 0.25 h; Microwave irradiationIonic liquid;
参考文献
Sharma, Nandini; Sharma, Upendra K.; Salwan, Richa; Kasana, Ramesh C.; Sinha, Arun K.
Catalysis Letters, 2011 , vol. 141, # 4 p. 616 - 622
反应条件
diisopropoxyaluminium trifluoroacetate; 4-nitrobenzaldehdye in benzene 0.25 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 38, # 39 p. 6925 - 6928
反应条件
dichloromethane extract derived from 6percent aqueous hypochlorite/tetra-n-butylammonium bisulfate solution with pH value to 8-9 in dichloromethane T=20°C;
参考文献
Synlett, , # 14 art. no. S03711ST, p. 2069 - 2071
反应条件
K5CoIIIW12O40; potassium acetate in water; acetic acid T=50°C; Yield given. Yields of byproduct given;
参考文献
European Journal of Organic Chemistry, , # 2 p. 299 - 302
反应条件
dichloromethane extract derived from 6percent aqueous hypochlorite/tetra-n-butylammonium bisulfate solution with pH value to 8-9 in dichloromethane T=20°C;
参考文献
Synlett, , # 14 art. no. S03711ST, p. 2069 - 2071