2'-溴-4-氯苯乙酮合成路线 （共 272 条）
反应条件
1,3-dibenzyl-1H-benzo[d]imidazol-3-ium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=20°C; 0.316667 h; Inert atmosphere;
参考文献
Singh, Santosh; Singh, Pankaj; Rai, Vijai K.; Kapoor, Ritu; Yadav, Lal Dhar S.
Tetrahedron Letters, 2011 , vol. 52, # 1 p. 125 - 128
参考文献
Lutz; Shearer
Journal of Organic Chemistry, 1947 , vol. 12, p. 771,773
反应条件
1: Na2S2O3*5H2O / H2O; ethanol / 0.25 h / Heating
2: 63 percent / I2 / 1 h / 19.9 °C
View Scheme
参考文献
Rymarczyk, Beate M.; Preut, Hans; Kreher, Richard P.
Acta Crystallographica Section C: Crystal Structure Communications, 1997 , vol. 53, # 7 p. 931 - 933
反应条件
in N,N-dimethyl-formamide
T=20°C;
参考文献
El'Tsov; Mokrushin; Smirnova; Shafikov
Russian Chemical Bulletin, 2011 , vol. 60, # 5 p. 882 - 888
反应条件
1: N,N-dimethyl-formamide
2: hydrogen bromide; acetic acid / water
View Scheme
参考文献
Li, Wen-Tai; Wu, Wan-Hsun; Tang, Chien-Hsiang; Tai, Ready; Chen, Shui-Tein
ACS Combinatorial Science, 2011 , vol. 13, # 1 p. 72 - 78
反应条件
potassium carbonate
20 h; Heating;
参考文献
Bernard, Angela M.; Piras, Pier P.
Synthetic Communications, 1997 , vol. 27, # 5 p. 709 - 723
反应条件
1: ethanol; H2O / 2 h / 20 °C
2: 45 percent / sulfur; morpholine / ethanol / 1 h / 70 °C
View Scheme
参考文献
Baraldi, Pier Giovanni; Zaid, Abdel Naser; Lampronti, Ilaria; Fruttarolo, Francesca; Pavani, Maria Giovanna; Tabrizi, Mojgan Aghazadhe; Shryock, John C.; Leung, Edward; Romagnoli, Romeo
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 17 p. 1953 - 1957
反应条件
1: 81 percent / S4N4*SbCl5 / toluene / 3.5 h / Heating
2: 82 percent / SbCl5 / CCl4 / 2 h / Heating
View Scheme
参考文献
Kim, Kil-Joong; Kim, Kyongtae
Tetrahedron Letters, 1997 , vol. 38, # 24 p. 4227 - 4230
反应条件
in nitrobenzene
T=70°C; varios solvents, reagents; crossover reactions;; Product distributionMechanism;
参考文献
Toeke, L.; Petnehazy, I.; Szakal, Gy.
Acta Chimica Academiae Scientiarum Hungaricae, 1981 , vol. 106, # 3 p. 179 - 184
反应条件
in isopropyl alcohol
参考文献
Chimenti, Franco; Bizzarri, Bruna; Maccioni, Elias; Secci, Daniela; Bolasco, Adriana; Fioravanti, Rossella; Chimenti, Paola; Granese, Arianna; Carradori, Simone; Rivanera, Daniela; Lilli, Daniela; Zicari, Alessandra; Distinto, Simona
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 16 p. 4635 - 4640
