反应条件
1: 1.) BuLi / 1.) ether, hexane, -78 deg C, 1.5 h, 2.) ether, hexane, a) -78 deg C, 1.5 h, b) RT, 10 h 2: 1.) DIBAL-H, 2.) NBS / 1.) hexane, RT, 10 h, 2.) 0 deg C 3: 1.) BuLi, 2.) (PhSO2)2S / 1.) ether, hexane, RT, 2 h, 2.) ether, hexane, RT, 20 h 4: 83 percent / TBAF / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Kurita, Jyoji; Ishii, Makoto; Yasuike, Shuji; Tsuchiya, Takashi
Journal of the Chemical Society, Chemical Communications, 1993 , # 17 p. 1309 - 1310
