1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane
T=0°C;
2: With zinc dibromide in tetrahydrofuran; hexane
T=0°C;
3: benzonitrile With n-tridecane; [NiCl2(PMe3)2] in tetrahydrofuran
T=65°C; 41 h; Further stages.;
参考文献
Penney, Jonathan M.; Miller, Joseph A.
Tetrahedron Letters, 2004 , vol. 45, # 25 p. 4989 - 4992