1,2-二苯基乙基-n-甲胺合成路线 （共 7 条）
反应条件
triethylamine in hexane; dichloromethane; cyclohexane; water
参考文献
Fisons Corporation
Patent: US5331007 A1, 1994 ;
反应条件
1: With Ind2TiMe2 in toluene
T=105°C; P=760 Torr; 7 h;
2: With sodium cyanoborohydride; zinc(II) chloride in methanol; toluene
T=25°C; 16 h;
参考文献
Marcsekova, Klaudia; Wegener, Bernd; Doye, Sven
European Journal of Organic Chemistry, 2005 , # 22 p. 4843 - 4851
反应条件
sodium hydroxide in tetrahydrofuran; water
参考文献
Fisons Corporation
Patent: US5047541 A1, 1991 ;
反应条件
formic acid
T=180°C;
参考文献
Goodson; Wiegand; Splitter
Journal of the American Chemical Society, 1946 , vol. 68, p. 2174
反应条件
sodium cyanoborohydride in methanol
72 h;
参考文献
Holzgrabe; Inkman
Archiv der Pharmazie, 1993 , vol. 326, # 4 p. 209 - 215
参考文献
Moffett; Hoehn
Journal of the American Chemical Society, 1947 , vol. 69, p. 1792
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Moffett
Org.Synth.Coll.Vol.IV<1963>605
反应条件
zinc in acetonitrile
1) cooling with an ice-salt bath -> room temperature, 5 h, 2) room temp., 2 days;
参考文献
Shono, Tatsuya; Hamaguchi, Hiroshi; Sasaki, Manji; Fujita, Shumei; Nagami, Kimihiko
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1621 - 1628
