3,3'-二-叔丁基-1,1'-联苯合成路线 （共 5 条）
反应条件
SSZ-55 zeolite
T=300°C; P=3750.38 Torr; 4 h; AutoclaveInert atmosphere; chemoselective reaction;
参考文献
Sugi, Yoshihiro; Maekawa, Hiroyoshi; Ito, Akira; Ozawa, Chikako; Shibata, Tomoko; Niimi, Amhiro; Asaoka, Chihara; Komura, Kenichi; Kubota, Yoshihiro; Lee, Jae-Youl; Kim, Jong-Ho; Seo, Gon
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 11 p. 2232 - 2242
反应条件
ethidium Bromide; magnesium
1) ether, reflux, 3 h, 2) reflux, 1 h; Yield given. Multistep reaction;
参考文献
Haefelinger, Guenter; Beyer, Michael
Liebigs Annalen der Chemie, 1980 , # 12 p. 2012 - 2020
反应条件
aluminium trichloride; 2,4-dimethylisopropylbenzene; benzene
T=34.9°C; 7 h; var. temp., time, ΔrHm0, ΔrSm0; Thermodynamic dataEquilibrium constant;
参考文献
Roshchupkina, I. Yu.; Nesterova, T. N.; Rozhnov, A. M.
Journal of Chemical Thermodynamics, 1987 , vol. 19, # 3 p. 299 - 306
反应条件
aluminium trichloride; tert-butyl benzene; benzene
T=34.9°C; var. temp.; Equilibrium constant;
参考文献
Roshchupkina, I. Yu.; Nesterova, T. N.; Rozhnov, A. M.
Journal of Chemical Thermodynamics, 1987 , vol. 19, # 3 p. 299 - 306
反应条件
aluminium trichloride in carbon disulfide
further products: 3,3',5,5'-tetra-tert-butylbiphenyl, 3-tert-butylbiphenyl, 4-tert-butylbiphenyl; determination of substitut. positions; Product distribution;
参考文献
Haefelinger, Guenter; Beyer, Michael
Liebigs Annalen der Chemie, 1980 , # 12 p. 2012 - 2020
