N-乙酰基-3-甲苯胺合成路线 （共 128 条）
反应条件
pyridinium dichlorobromate; alpha-cyclodextrin in water
T=20°C; 1 h; Product distribution; Further Variations:Reagents;
参考文献
Dumanski, Paul G.; Easton, Christopher J.; Lincoln, Stephen F.; Simpson, Jamie S.
Australian Journal of Chemistry, 2003 , vol. 56, # 11 p. 1107 - 1111
反应条件
trichlorophosphate in 1,2-dichloro-ethane
4.5 h; Heating;
参考文献
Meth-Cohn, Otto; Narine, Brahma; Tarnowski, Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1531 - 1536
反应条件
1: acetic acid; acetic acid anhydride; nitric acid / und Erhitzen des Reaktionsprodukts mit wss.Schwefelsaeure
2: pyridine
3: aqueous NaOH-solution
4: acetic acid; sulfuric acid
5: palladium; ethanol / Hydrogenation
6: sodium hydrogencarbonate; diethyl ether
7: toluene
View Scheme
参考文献
Green; Day
Journal of the American Chemical Society, 1942 , vol. 64, p. 1167,1170
反应条件
1: acetic acid; acetic acid anhydride; nitric acid / und Erhitzen des Reaktionsprodukts mit wss.Schwefelsaeure
2: pyridine
3: aqueous NaOH-solution
4: acetic acid; sulfuric acid
View Scheme
参考文献
Green; Day
Journal of the American Chemical Society, 1942 , vol. 64, p. 1167,1170
反应条件
dipotassium peroxodisulfate; methanesulfonic acid; palladium diacetate in ethylene glycol dimethyl ether
T=25°C; 24 h;
参考文献
Jiang, Tao-Shan; Wang, Guan-Wu
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9504 - 9509,6
反应条件
AcOF in dichloromethane; monofluoro-trichloromethane
T=-75°C;
参考文献
Lerman, Ori; Yitzhak, Tor; Hebel, David; Rozen, Shlomo
Journal of Organic Chemistry, 1984 , vol. 49, p. 806 - 813
反应条件
1: (i) (bromination), (ii) (hydrolysis)
2: (i) NaNO2, aq. HCl, (ii) /BRN= 3587244/
3: (i) Mg, Et2O, (ii) iPrBr, (iii) (heating), aq. H2SO4
View Scheme
参考文献
Nasipuri,D. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1979 , p. 3034 - 3036
反应条件
nitrogen(IV) oxide; ozone in chloroform
2 h; < 0 deg C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Suzuki, Hitomi; Tatsumi, Atsuo; Ishibashi, Taro; Mori, Tadashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 339 - 344
参考文献
Borsche
Justus Liebigs Annalen der Chemie, 1908 , vol. 359, p. 76
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Cohen; Dakin
Journal of the Chemical Society, 1903 , vol. 83, p. 331
参考文献
Beilstein; Kuhlberg
Justus Liebigs Annalen der Chemie, 1871 , vol. 158, p. 347
Show Details
Cohen; Dakin
Journal of the Chemical Society, 1903 , vol. 83, p. 331
