3-苯氧基-1,2-丙二醇合成路线 (共 55 条)
反应条件
1: 2.) 50percent aq. NaOH / 1.) 80 deg C, 2.) 4 h 2: 78 percent / 72percent HClO4 / H2O / 80 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 105, # 3 p. 586 - 593
反应条件
Py(HF)x in acetonitrile T=20°C; 4 h; Product distribution;
参考文献
Watanabe, Yutaka; Kiyosawa, Youko; Tatsukawa, Akiko; Hayashi, Minoru
Tetrahedron Letters, 2001 , vol. 42, # 28 p. 4641 - 4643
反应条件
N-bromosuccinmide; ammonium cerium(IV) nitrate in water; acetonitrile T=20°C;
参考文献
Tetrahedron Letters, , vol. 46, # 23 p. 4111 - 4113
反应条件
Bacillus megaterium ECU1001 epoxide hydrolase in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 0.0833333 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zhao, Jing; Chu, Yan-Yan; Li, Ai-Tao; Ju, Xin; Kong, Xu-Dong; Pan, Jiang; Tang, Yun; Xu, Jian-He
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1510 - 1518
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium hydrogencarbonate in 1,4-dioxane T=90°C; Addition; ring cleavage;
参考文献
Tetrahedron, , vol. 53, # 13 p. 4787 - 4790
反应条件
5 palladium on charcoal in neat (no solvent) T=130°C; 24 h; Inert atmosphereGreen chemistry; Time;
参考文献
Green Chemistry, , vol. 15, # 2 p. 347 - 352
反应条件
β-glucuronidase; arylsulfatase from Helix pomatia in methanol T=37°C; 24 h; pH = 4.6;
参考文献
Archiv der Pharmazie, , vol. 323, # 5 p. 259 - 265
反应条件
zirconium tetrakis(dodecyl sulfate); water T=50°C;
参考文献
Helvetica Chimica Acta, , vol. 93, # 3 p. 405 - 413
反应条件
sodium hydroxide in isopropyl alcohol T=100°C; 1 h;
参考文献
Rokicki, G.; Pawlicki, J.; Kuran, W.
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 5 p. 718 - 722
反应条件
potassium carbonate T=110°C; 2 h;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 327, # 5 p. 718 - 722