1: With iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride in tetrahydrofuran T=-20°C; 0.25 h; 2: With LiH3BNMe2 in tetrahydrofuran T=-20 - 20°C; 16 h;
参考文献
Chemical Communications, , vol. 48, # 10 p. 1580 - 1582
water-d2; diisobutylaluminium hydride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride 1) THF, -78 deg C to 0 deg C, 24 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 25 p. 6188 - 6194
water-d2; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in diethyl ether T=-78 - 0°C; 24 h; without catalyst, other solvent, other reaction temperatures; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 55, # 25 p. 6188 - 6194
