1-(4-氯苯基)-1,4-戊二酮合成路线 （共 37 条）
反应条件
9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene
24 h; Heating; Title compound not separated from byproducts.;
参考文献
Pridmore, Simon J.; Slatford, Paul A.; Daniel, Aurelie; Whittlesey, Michael K.; Williams, Jonathan M.J.
Tetrahedron Letters, 2007 , vol. 48, # 29 p. 5115 - 5120
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
24 h; Reflux;
参考文献
O'Reilly, Elaine; Iglesias, Cesar; Ghislieri, Diego; Hopwood, Jennifer; Galman, James L.; Lloyd, Richard C.; Turner, Nicholas J.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2447 - 2450
Angew. Chem., 2014 , vol. 53, # 9 p. 2479 - 2482,4
反应条件
air; acetic acid
T=23°C; 12 h; Further byproducts given;
参考文献
Nishino, Hiroshi; Tategami, Shin-ichi; Yamada, Takashi; Korp, James D.; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 6 p. 1800 - 1809
反应条件
1: aq. NaOH
2: (i) Ac2O, (ii) /BRN= 506021/, Et3N, CH2Cl2, (iii) aq. NaOH
View Scheme
参考文献
Nimgirawath,S. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 339 - 356
反应条件
(i) Ac2O, (ii) /BRN= 506021/, Et3N, CH2Cl2, (iii) aq. NaOH; Multistep reaction;
参考文献
Nimgirawath,S. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 339 - 356
反应条件
molecular sieve in benzene
2 h; Heating / reflux;
参考文献
LUPIN LIMITED
Patent: WO2004/26828 A1, 2004 ;
Location in patent: Page 25 ;
反应条件
phenylammonium bromide in ethanol
3 h; Heating;
参考文献
Cerreto; Villa; Retico; Scalzo
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 7 p. 701 - 708
