1-(4-溴苯基)-1-乙醇合成路线 (共 105 条)
反应条件
in 1,4-dioxane; water 168 h; Reflux;
参考文献
Chemistry - A European Journal, , vol. 19, # 1 p. 314 - 323
反应条件
in hydrogenchloride; ethanol; butan-1-ol Ambient temperaturecathode: Pb plate (ca. 21.3 cm2); Pt plate (ca. 4.0 cm2), constant current density (-3.7 mA/cm2);
参考文献
Chemistry Letters, , # 9 p. 1719 - 1720
反应条件
trimethyltelluronium iodide 1.) hexane, THF, -60 deg C, 10 min, 2.) -78 deg C -> RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2847 - 2848
反应条件
n-butyllithium 1.) hexane, THF, -60 deg C, 10 min, 2.) -78 deg C -> RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2847 - 2848
参考文献
Chemische Berichte, , vol. 55, p. 3414
Bulletin de la Societe Chimique de France, , vol. <4> 45, p. 78
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 182, p. 1284
反应条件
Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 1631,1634
反应条件
Hydrogenation; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 22, p. 93
反应条件
in acetone T=25°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 35, # 47 p. 8751 - 8754
反应条件
tris-imidazolium-stabilized palladium; potassium carbonate in water; toluene T=90°C; Suzuki coupling; 4.5 h;
参考文献
Planellas, Marc; Pleixats, Roser; Shafir, Alexandr
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 651 - 662
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 63°C; 3 h;
参考文献
Yasuda; Onishi; Ueba; Miyai; Baba
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7741 - 7744