1,2-丙二烯三正丁基锡合成路线 （共 51 条）
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Veerman, Johan J. N.; Rutjes, Floris P. J. T.; Van Maarseveen, Jan H.; Hiemstra, Henk
Tetrahedron Letters, 1999 , vol. 40, # 33 p. 6079 - 6082
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in N,N-dimethyl-formamide T=25°C; 12 h;
参考文献
Huang, Chih-Wei; Shanmugasundaram, Muthian; Chang, Hao-Ming; Cheng, Chien-Hong
Tetrahedron, 2003 , vol. 59, # 20 p. 3635 - 3641
反应条件
1: (Z)-3-iodo-3-methylpropenoic acid With tetrabutylammomium bromide; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=20°C; 0.166667 h; 2: allenyl tributylstannane in N,N-dimethyl-formamide 4 h;
参考文献
Rousset; Abarbri; Thibonnet; Duchene; Parrain
Chemical Communications, 2000 , # 20 p. 1987 - 1988
反应条件
isomerization on storing (more than three months);
参考文献
Boaretto, Andrea; Marton, Daniele; Tagliavini, Giuseppe
Journal of Organometallic Chemistry, 1985 , vol. 297, p. 149 - 154
参考文献
Moriya, Osamu; Urata, Yoshikiyo; Endo, Takeshi
Journal of the Chemical Society, Chemical Communications, 1991 , # 13 p. 884 - 885
反应条件
in neat (no solvent) GeCl3 was introduced into a N2-filled flask, Sn-compound was slowly added at room temp., the mixt. was stirred for 30 min at 50°C; selective condensation in a trap cooled at -30°C, kept in a freezer (-20°C);
参考文献
Strenalyuk, Tatyana; Samdal, Svein; Mollendal, Harald; Guillemin, Jean-Claude
Journal of Molecular Structure, 2006 , vol. 780-781, # SPEC. ISS. p. 157 - 162
反应条件
methyllithium 1) THF, -95 deg C, 10 min 2) -95 deg C, 20 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Suzuki, Masaaki; Morita, Yasushi; Noyori, Ryoji
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 441 - 449
反应条件
in dichloromethane T=0 - 20°C; 5 h;
参考文献
Chemistry Letters, , p. 1519 - 1522
反应条件
titanium tetrachloride in dichloromethane
T=-78°C; Yield given;
参考文献
Haruta, Jun-ichi; Nishi, Koichi; Matsuda, Satoshi; Akai, Shuji; Tamura, Yasumitsu; Kita, Yasuyuki
Journal of Organic Chemistry, 1990 , vol. 55, # 16 p. 4853 - 4859
反应条件
methyllithium
1) THF, -95 deg C, 10 min 2) -95 deg C, 20 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Suzuki, Masaaki; Morita, Yasushi; Noyori, Ryoji
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 441 - 449
