2,2,6-三甲基-4H-1,3-二英-4-酮合成路线 （共 203 条）
参考文献
Sato, Masayuki; Ogasawara, Hiromischi; Kato, Keiko; Sakai, Masako; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4300 - 4305
参考文献
Sato, Masayuki; Ogasawara, Hiromischi; Kato, Keiko; Sakai, Masako; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4300 - 4305
反应条件
in xylene
0.5 h; Heating;
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
反应条件
sodium acetate in tetrahydrofuran
24 h; Reflux;
参考文献
Li, Suhua; Chen, Gang; Feng, Chen-Guo; Gong, Wei; Yu, Jin-Quan
Journal of the American Chemical Society, 2014 , vol. 136, # 14 p. 5267 - 5270
反应条件
in xylene
T=140 - 145°C; 1 h;
参考文献
Gorlitzer; Baltrusch
Pharmazie, 2000 , vol. 55, # 10 p. 747 - 750
反应条件
diisobutylaluminium hydride; toluene-4-sulfonic acid
1.) irradiation, hexane, 24 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Baldwin, S. W.; Wilkinson, J. M.
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3634 - 3635
反应条件
in xylene
0.5 h; Heating;
参考文献
Mueller, Paul; Polleux, Philippe
Helvetica Chimica Acta, 1994 , vol. 77, p. 645 - 654
反应条件
1: 2,2,6-trimethyl-4H-1,3-dioxin-4-one With dihydroxy-poly(ethylene glycol) of MW = 4000 in toluene
5 h; Heating;
2: α-(3-Hydroxyphenoxy)acetophenone With titanium tetrachloride in tetrahydrofuran
T=20°C; von Pechmann reaction; 0.5 h;
参考文献
Sheng, Shou-Ri; Huang, Pei-Gang; Wang, Qiong; Huang, Ren; Liu, Xiao-Ling
Synthetic Communications, 2006 , vol. 36, # 21 p. 3175 - 3181
反应条件
in xylene
T=150°C; 0.5 h;
参考文献
Clemens, Robert J.; Hyatt, John A.
Journal of Organic Chemistry, 1985 , vol. 50, # 14 p. 2431 - 2435
反应条件
in anhydrous xylene
T=145°C; 0.5 h; Inert atmosphere;
参考文献
Xin, Dongyue; Burgess, Kevin
Organic Letters, 2014 , vol. 16, # 8 p. 2108 - 2110
