1-(苯基亚甲基)-1H-茚合成路线 (共 12 条)
反应条件
An2TeO in acetonitrile
17 h; Ambient temperatureIrradiation;
参考文献
Zheng, Ming; Wang, Longcheng; Shao, Jianguo; Zhong, Qi
Synthetic Communications, 1997 , vol. 27, # 10 p. 1751 - 1755
反应条件
samarium; samarium diiodide in tetrahydrofuran
T=67°C; 4 h;
参考文献
Ogawa, Akiya; Takami, Noriaki; Nanke, Taizoh; Ohya, Syoji; Hirao, Toshikazu; Sonoda, Noboru
Tetrahedron, 1997 , vol. 53, # 38 p. 12895 - 12902
反应条件
potassium fluoride on basic alumina in methanol
T=65°C; 8 h;
参考文献
Lu, Wenxing; Zhu, Quan; Yan, Chao-Guo
Synthetic Communications, 1997 , vol. 27, # 22 p. 3985 - 3990
反应条件
1: tetrahydrofuran / -78 °C
2: 50 percent / MeI / -25 °C
View Scheme
参考文献
Woning, Jan; Lijten, Frank A. T.; Laarhoven, Wim H.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2427 - 2435
反应条件
1: tetrahydrofuran / -78 °C
2: 50 percent / MeI / -25 °C
View Scheme
参考文献
Woning, Jan; Lijten, Frank A. T.; Laarhoven, Wim H.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2427 - 2435
反应条件
methyl iodide
T=-25°C;
参考文献
Woning, Jan; Lijten, Frank A. T.; Laarhoven, Wim H.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2427 - 2435
反应条件
chloroform; bromine
ω-phenyl-benzofulvene;
参考文献
Courtot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1915 , vol. 160, p. 523
Annales de Chimie (Cachan, France), 1915 , vol. <9> 4, p. 114,127
反应条件
hydrogenchloride
Behandlung des Reaktionsproduktes mit Pyridin; ω-phenyl-benzofulvene;
参考文献
Courtot
Annales de Chimie (Cachan, France), 1915 , vol. <9> 4, p. 205
反应条件
1: diethyl ether
2: bromine; chloroform
View Scheme
参考文献
Courtot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1915 , vol. 160, p. 523
Annales de Chimie (Cachan, France), 1915 , vol. <9> 4, p. 114,127
反应条件
T=700°C; 8.33333E-05 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hofmann, Joerg; Schulz, Kathrin; Altmann, Annett; Findeisen, Matthias; Zimmermann, Gerhard
Liebigs Annales, 1997 , # 12 p. 2541 - 2548