2,3-二苯基-1,4-二氮杂螺[4.5]癸-1,3-二烯合成路线 （共 2 条）
反应条件
ammonium acetate in acetic acid
T=118°C;
参考文献
Zhou, Yan; Andreou, Anna; Biktagirov, Eldar; Eames, Jason; Wadhawan, Jay
Electrochemistry Communications, 2010 , vol. 12, # 11 p. 1493 - 1497
反应条件
1: Grubb's 2nd generation catalyst; tetra-(n-butyl)ammonium iodide; tert.-butylhydroperoxide / toluene; acetonitrile; water / 1 h / 20 °C / |Inert atmosphere
2: ammonium acetate / acetic acid / 2 h / 100 °C / |Inert atmosphere
View Scheme
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
