chlorine byproducts: NaCl; dry NaSCN is filled in a drying tower, then a stream of dry chlorine is passed slowly through the tower at room temp. (under nitrogen); residual chlorine is displaced by nitrogen, the product is extracted from the tower, washed with acetone and then extracted for 24 h in a Soxhlet apparatus with MeOH and further 24 h with acetone, the product is left in vac. for some days, elem. anal.;
参考文献
Cataldo, Franco; Fiordiponti, Paolo
Polyhedron, 1993 , vol. 12, p. 279 - 284
