Drach, B. S.; Popovich, T. P.; Kalinin, V. N.; Kisilenko, A. A.; Soifer, G. B.; Gordeev, A. D.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 640 - 647
Zhurnal Organicheskoi Khimii, 1984 , vol. <4> 20, p. 704 - 712
1: sodium isothiocyanate; benzoyl chloride in acetone
T=0°C; Substitution;
2: 3-nitro-aniline in acetone
T=20°C; Addition;
参考文献
Chan, Chung Woo; Ng, Chun Ming Dominic; Ho, Joyce; Tin, Kam Chung
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 3 p. 216 - 219
in chloroform; acetonitrile
byproducts: NaCl; ICl in CH3CN added over 10-20 min to NaNCS in CH3CN at -10°C under stirring, stirred for 5-10 min, filtered, CHCl3 added, at room temp. Ph3SnCl added dropwise under stirring, refluxed for 2 h; filtered, concd., distilled at 10 mm/Hg, residue crystd. by addition of ether, washed (ether), dried at 30°C/10 mm/Hg; elem. anal.;
参考文献
Srivastava; Tangri
Journal of the Indian Chemical Society, 1991 , vol. 68, # 10 p. 560 - 562
1: sodium isothiocyanate; benzoyl chloride in acetone
T=0°C; Substitution;
2: N-methylaniline in acetone
T=20°C; Addition;
参考文献
Chan, Chung Woo; Ng, Chun Ming Dominic; Ho, Joyce; Tin, Kam Chung
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 3 p. 216 - 219
