反应条件
hydrogenchloride; n-butyllithium; diisopropylamine in tetrahydrofuran Ar-atmosphere; dropwise addn. of BuLi to diisopropylamine (-78°C), addn. to B(O-iPr)3 and CH2Cl2, stirring (15 min, -78°C), bubbling of HCl to methyl orange endpoint; filtration off of iPr2NH*HCl, washing (ether), evapn. of solvents (vac., below 45°C), distn. (vac.);
参考文献
Matteson, Donald S.; Hurst, Gerald D.
Organometallics, 1986 , vol. 5, p. 1465 - 1467
