oxonium; magnesium in tetrahydrofuran Sonication; 1. THF/I; 2. H3O(1+), supersonic wave; according to: V. Percec, T. K. Bera, B. B. De, Y. Sanai, J. Smith, M. N. Holerca, B. Barboiu, R. B. Grubbs, J. M. J. Frechet, J. Org, Chem. 66 (2001) 2104;
1: 1-bromo-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]benzene With n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h; 2: tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C; Further stages.;
1: 2-methoxybromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78 - -10°C; 2: tri-isopropoxy-borane in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Lloyd, David G.; Hughes, Rosario B.; Zisterer, Daniela M.; Williams, D. Clive; Fattorusso, Caterina; Catalanotti, Bruno; Campiani, Giuseppe; Meegan, Mary J.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 23 p. 5612 - 5615
