反应条件
C4H9Li; HCl in tetrahydrofuran; hexane addn. of hexane soln. of butyllithium to THF soln. of benzene deriv. at -78°C, stirring for 20 min at -78°C under Ar, addn. of borate deriv., stirring for 1 h at -78°C, warming to room temp.; addn. of diethyl ether and water, addn. of aq. HCl to pH 7, separation of organic layer, extn. of aq. soln. (diethyl ether), evapn. of combined organic solns., chromy. (silica gel, toluene/acetone (4:1)), NMR;
参考文献
Collin, Jean-Paul; Durola, Fabien; Lux, Jacques; Sauvage, Jean-Pierre
New Journal of Chemistry, 2010 , vol. 34, # 1 p. 34 - 43
