1,2-乙二醇单乙酸酯合成路线 （共 112 条）
反应条件
HY-Zeolite in chloroform 2 h; Heating;
参考文献
Srinivas; Mahender; Das, Biswanath
Synlett, 2003 , # 15 p. 2419 - 2421
反应条件
1: 3-(2-acetaminoethyl)indole With triphenyl phosphite; chlorine; triethylamine in dichloromethane T=-30°C; 2: ethylene glycol in dichloromethane T=-30 - 20°C; 3: With water
参考文献
Spaggiari, Alberto; Blaszczak, Larry C.; Prati, Fabio
Organic Letters, 2004 , vol. 6, # 22 p. 3885 - 3888
反应条件
1: N-(cyclohexyl)acetamide With triphenyl phosphite; chlorine; triethylamine in dichloromethane T=-30°C; 2: ethylene glycol in dichloromethane T=-30 - 20°C; 3: With water
参考文献
Spaggiari, Alberto; Blaszczak, Larry C.; Prati, Fabio
Organic Letters, 2004 , vol. 6, # 22 p. 3885 - 3888
反应条件
1: N-(1-phenylethyl)acetamide With triphenyl phosphite; chlorine; triethylamine in dichloromethane T=-30°C; 2: ethylene glycol in dichloromethane T=-30 - 20°C; 3: With water
参考文献
Spaggiari, Alberto; Blaszczak, Larry C.; Prati, Fabio
Organic Letters, 2004 , vol. 6, # 22 p. 3885 - 3888
反应条件
1: (S)-N-acetyl-1-phenylethylamine With triphenyl phosphite; chlorine; triethylamine in dichloromethane T=-30°C; 2: ethylene glycol in dichloromethane T=-30 - 20°C; 3: With water
参考文献
Spaggiari, Alberto; Blaszczak, Larry C.; Prati, Fabio
Organic Letters, 2004 , vol. 6, # 22 p. 3885 - 3888
反应条件
1: With sodium hydride T=20°C; 1.5 h; 2: With phosphoric acid in water Product distribution / selectivity;
参考文献
LEK PHARMACEUTICALS D.D.; UDOVIC, Marko; TRAMSEK, Marko; PLANTAN, Ivan; CLUZEAU, Jerome
Patent: WO2011/64249 A1, 2011 ;
Location in patent: Page/Page column 23 ;
反应条件
hydrogen; ruthenium(IV) oxide T=220°C; P=326800 Torr; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 103, # 13 p. 3959 - 3961
反应条件
sodium hydrogen sulphate in hexane T=50°C; 5 h;
参考文献
Journal of the American Chemical Society, , vol. 111, # 25 p. 9102 - 9103
反应条件
(10H)-phenothiazine; chromium (III) ethanoate T=60 - 80°C; P=750.075 Torr; 6.1 h; Autoclave;
参考文献
US2004/30180 A1, ;
Page 9-11 ;
反应条件
H2 in methyl acetate; water; ethyl acetate
