1,2-乙二醇单乙酸酯合成路线 （共 112 条）
反应条件
hydrogenchloride; phosphate buffer; water T=25°C; rate and equilibrium constant of hydrolysis, at ionic strength 0.1; Product distributionKineticsMechanism;
参考文献
Journal of the American Chemical Society, , vol. 110, # 9 p. 2909 - 2914
反应条件
pyridine T=37°C; 10 h; pronase E (proteases from Streptomyces griseus);
参考文献
Bhattacharya, A; Ali, E
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 12 p. 898 - 899
反应条件
iodine; oxygen T=140°C; 1.5 h; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 10 p. 3200 - 3204
反应条件
sodium hydroxide; 4 A molecular sieve; silver carbonate 1.) CH2Cl2, room temp. 2.) reflux, 2 h; Yield given. Multistep reaction;
参考文献
Aitken, David J.; Rees, Lilias; Suckling, Colin J.; Wood, Hamish C. S.
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3417 - 3420
反应条件
Ala281Val mutated Candida antarctica lipase B immobilized on Accurel beads in tert-butyl methyl ether Enzymatic reaction;
参考文献
Chemical Communications, , vol. 48, # 80 p. 10013 - 10015
反应条件
sodium hydroxide; 4 A molecular sieve; silver carbonate 1.) CH2Cl2, room temp. 2.) reflux, 2 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Aitken, David J.; Rees, Lilias; Suckling, Colin J.; Wood, Hamish C. S.
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3417 - 3420
反应条件
sodium hydroxide; 4 A molecular sieve; silver carbonate 1.) CH2Cl2, room temp. 2.) reflux, 2 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Aitken, David J.; Rees, Lilias; Suckling, Colin J.; Wood, Hamish C. S.
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3417 - 3420
反应条件
Ala281Glu mutated Candida antarctica lipase B immobilized on Accurel beads in tert-butyl methyl ether Enzymatic reaction; Reagent/catalyst;
参考文献
Chemical Communications, , vol. 48, # 80 p. 10013 - 10015
反应条件
sodium hydroxide; 4 A molecular sieve; silver carbonate 1.) CH2Cl2, room temp. 2.) reflux, 2 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Aitken, David J.; Rees, Lilias; Suckling, Colin J.; Wood, Hamish C. S.
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3417 - 3420
反应条件
sodium hydroxide; 4 A molecular sieve; silver carbonate 1.) CH2Cl2, room temp. 2.) reflux, 2 h; Yield given. Multistep reaction;
参考文献
Aitken, David J.; Rees, Lilias; Suckling, Colin J.; Wood, Hamish C. S.
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3417 - 3420
