2,6-di-tert-butyl-pyridine; lt;(η5-C5H5)Fe(H2C=CH-CHO)(BIHOP-F)gt;lt;BF4gt; in dichloromethane T=-30°C; 16 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bruin, Marion E.; Peter Kuendig
Chemical Communications, 1998 , # 23 p. 2635 - 2636
n-butyllithium; methyllithium 1) dimethyl ether, -35 deg C to -30 deg C, 30 min, 2) dimethyl ether, ether, -35 deg C to -30 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;