hydrogen; palladium on activated charcoal in acetic acid P=735.5 Torr; 36 h; Ambient temperature;

acetone

1: 67 percent / sulphuryl chloride / acetic acid / 0.5 h / 50 °C 2: 1.) tetrabutylammonium bromide, 30percent aq. potassium hydroxide / 1.) chloroform, 20 deg C, 1 h, 2.) irradiation, 3 h 3: 89 percent / H2 / 10percent palladium-carbon / acetic acid / 36 h / 735.5 Torr / Ambient temperature View Scheme

1: 1.) tetrabutylammonium bromide, 30percent aq. potassium hydroxide / 1.) chloroform, 20 deg C, 1 h, 2.) irradiation, 3 h 2: 89 percent / H2 / 10percent palladium-carbon / acetic acid / 36 h / 735.5 Torr / Ambient temperature View Scheme

ethanol; platinum

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暂无反应条件数据

potassium hydrogensulfate; xylene

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