2,4-二氯-6-甲基嘧啶合成路线 （共 66 条）
参考文献
Claesen; Vanderhaeghe
Bulletin des Societes Chimiques Belges, 1959 , vol. 68, p. 30,55
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C;
参考文献
Baumann, Karlheinz; Flohr, Alexander; Goetschi, Erwin; Jacobsen, Helmut; Jolidon, Synese; Luebbers, Thomas
Patent: US2009/215759 A1, 2009 ;
Location in patent: Page/Page column 49 ;
反应条件
N-ethyl-N,N-diisopropylamine in ethanol 1.) 0 deg C, 3 h, 2.) 25 deg C, 24 h, 3.) reflux, 1 h;
参考文献
DuPont Pharmaceuticals Company
Patent: US6342503 B1, 2002 ;
Location in patent: Example 4 ;
US 6342503 B1
反应条件
1: alcohol; ammonia / im Rohr 2: concentrated hydriodic acid; red phosphorus View Scheme
参考文献
Gabriel; Colman
Chemische Berichte, 1899 , vol. 32, p. 2934
Chemische Berichte, 1902 , vol. 35, p. 1570
反应条件
ethanol; ammonia T=100°C; im Rohr;
参考文献
Chemische Berichte, , vol. 32, p. 2934
Chemische Berichte, , vol. 35, p. 1570
参考文献
Marshall; Walker
Journal of the Chemical Society, 1951 , p. 1004,1015
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, vol. 24, p. 84
参考文献
Chemische Berichte, , vol. 32, p. 2934
Chemische Berichte, , vol. 35, p. 1570
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C;
参考文献
US2009/215759 A1, ;
Page/Page column 50 ;
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C;
参考文献
US2009/215759 A1, ;
Page/Page column 49 ;
反应条件
1: NH3 2: palladium/charcoal; methanol / Hydrogenation View Scheme
参考文献
Gabriel; Colman
Chemische Berichte, 1899 , vol. 32, p. 2934
Chemische Berichte, 1902 , vol. 35, p. 1570
