1,4-二氧杂-2-己烯合成路线 (共 23 条)
反应条件
oxygen in tetrachloromethane T=-5°C; P=7600 Torr; 4 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 27, # 26 p. 2953 - 2956
反应条件
oxygen in tetrachloromethane T=-5°C; P=7600 Torr; 6 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 27, # 26 p. 2953 - 2956
反应条件
(i) O2, (ii) (thermolysis); Multistep reaction;
参考文献
Schaap,A.P.
Tetrahedron Letters, 1971 , p. 1757 - 1760
反应条件
tert.-butyl lithium in tetrahydrofuran T=-30°C;
参考文献
Fetizon, Marcel; Goulaouic, Pierre; Hanna, Issam
Tetrahedron Letters, 1985 , vol. 26, # 40 p. 4925 - 4928
反应条件
tert.-butyl lithium in tetrahydrofuran T=-30°C;
参考文献
Fetizon, Marcel; Goulaouic, Pierre; Hanna, Issam
Tetrahedron Letters, 1985 , vol. 26, # 40 p. 4925 - 4928
反应条件
in dichloromethane T=-20°C; 1 h;
参考文献
Adam, Waldemar; Andler, Simone; Heil, Markus
Angewandte Chemie, 1991 , vol. 103, # 10 p. 1395 - 1396
参考文献
Diveley et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 139,143
反应条件
hydrogenchloride; water in propan-1-ol T=95°C; var. conc.; Rate constant;
参考文献
Tsivunin, V. S.; Nasybullin, Sh. A.; Zaripova, V. G.; Ismagilov, R. M.; Zaripov, I. N.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 7 p. 1379 - 1382
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 7 p. 1529 - 1533
反应条件
n-butyl-magnesium bromide; zinc(II) chloride; benzene
Reagens 4: Aether;
参考文献
Summerbell; Umhoefer
Journal of the American Chemical Society, 1939 , vol. 61, p. 3016,3017
反应条件
n-butyllithium in hexane
T=0°C; 2 h;
参考文献
Saylor, Richard W.; Sebastian, John F.
Synthetic Communications, 1982 , vol. 12, # 8 p. 579 - 584